並列タイトル等Study on Thermal Decomposition Characteristic of FOX-12 based on Thermal Analysis with in-situ Observation and Spectroscopic Analysis
タイトル（掲載誌）宇宙航空研究開発機構研究開発報告: 高エネルギー物質研究会: 令和2年度研究成果報告書 = JAXA Research and Development Report: Technical Report of The Research Activity for High Energy Materials (2020)
一般注記Guanylurea dinitramide which is usually called FOX-12 is typical dinitramide salts. To obtain better understanding of thermal decomposition characteristic of FOX-12, this paper focused on analysis of initial decomposition of FOX-12 using in situ measurement with differential scanning calorimetry (DSC) and sample observation or Raman spectrometry for understanding decomposition characteristic of FOX-12. We conducted Raman spectroscopic analysis and sample observation during thermal analysis at 1 and 8 C min-1. The experiment results found that thermal behavior of FOX-12 was different by heating rate and formed condensed phase before sharp exotherm at high heating rate. For DSC/Raman result indicated guanidium nitrate (GN) and cyanuric acid formed during thermal decomposition of FOX-12. From observation results, GN and cyanuric acid formed with solid phase reaction of initial decomposition. And the molten GN affects the precipitous exothermal reaction of FOX-12.
形態: カラー図版あり
Physical characteristics: Original contains color illustrations
資料番号: AA2030016006
レポート番号: JAXA-RR-20-007
連携機関・データベース国立情報学研究所 : 学術機関リポジトリデータベース（IRDB）（機関リポジトリ）
提供元機関・データベース宇宙航空研究開発機構 : 宇宙航空研究開発機構リポジトリ