Synthesis and Characterization of LiNi_<0.5>Mn_<1.5.O_4 Particles by Internal Combustion Type Spray Pyrolysis and Spray Drying

Material type: 文書・図像類

Author: MYOUJIN, Kenichiほか

Publisher: 日本MRS

Publication date: 2008-11

Material Format: Digital

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Note (General)：: Spherical LiNi_<0.5>Mn_<1.5>O_4 precursor powders were synthesized different heating method by internal combustion type spray pyrolysis apparatus usi...

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Material Type: 文書・図像類
Title: Synthesis and Characterization of LiNi_<0.5>Mn_<1.5.O_4 Particles by Internal Combustion Type Spray Pyrolysis and Spray Drying
Author/Editor: MYOUJIN, Kenichi
KOJIMA, Masayuki
OGIHARA, Takashi
NAKANE, Koji
OGATA, Nobuo
Author Heading: MYOUJIN, Kenichi
KOJIMA, Masayuki
OGIHARA, Takashi
NAKANE, Koji
OGATA, Nobuo
Publication, Distribution, etc.: 日本MRS
Publication Date: 2008-11
Publication Date (W3CDTF): 2008-11
Periodical title: Transactions of the Materials Research Society of Japan
No. or year of volume/issue: 33 4
Volume: 33
Issue: 4
Pages: 985-988
ISSN (Periodical Title): ISSN : 1382-3469
Text Language Code: eng
Subject Heading: Lithium Manganese Oxides
Lithium Secondary Battery
Spinel
Spray Pyrolysis
Spray Drying
Target Audience: 一般
Note (General): Spherical LiNi_<0.5>Mn_<1.5>O_4 precursor powders were synthesized different heating method by internal combustion type spray pyrolysis apparatus using gas burner. After calcinations of as-prepared powders contained Ni at different temperatures from 800 to 1200 ℃ in air for 10h, LiNi_<0.5>Mn_<1.5>O_4 powders were obtained. As-prepared particles have a porous microstructure with an average diameter of about 5 μm (spray pyrolysis) and 2 μm (spray drying) with narrow size distribution. The powder production capacity was 1 kg/h by this equipment. XRD showed that LiNi_<0.5>Mn_<1.5>O_4 powders were well crystallized to a spinel structure with Fd3m space group. LiNi_<0.5>Mn_<1.5>O_4 powders calcined at 1000 ℃ shows good cycle performance with initial discharge capacity of 130 mAh/g and 93 % retention after 300 cycles between 3.5 V and 5.0 V. The most of electrochemical properties of LiNi_<0.5>Mn_<1.5>O_4 powders that spray drying method offered superior performance to spray pyrolysis method.
Source: https://u-fukui.repo.nii.ac.jp/?action=repository_action_common_download&item_id=22596&item_no=1&attribute_id=22&file_no=1
https://u-fukui.repo.nii.ac.jp/?action=repository_action_common_download&item_id=22596&item_no=1&attribute_id=22&file_no=1
Access Restrictions: 限定公開
Rights (production): 日本MRS
Data Provider (Database): 国立情報学研究所 : 学術機関リポジトリデータベース（IRDB）（機関リポジトリ）
https://irdb.nii.ac.jp
Original Data Provider (Database): 福井大学 : 福井大学学術機関リポジトリ