脱水縮合反応を志向した新規骨格を有する電子欠乏性含窒素芳香環の開発

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Author: 國嶋, 崇隆ほか

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Publication date: 2017-05-24

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Note (General)：: 金沢大学医薬保健研究域薬学系脱水縮合剤DMT-MMは、水中やアルコール中でもカルボン酸とアミンの脱水縮合反応が選択的に進行し、アミドを高収率に与える優れた縮合剤である。今回、DMT-MMを構成するπ電子欠乏性トリアジン環の置換基検討と骨格変換を行うことで、複数の新規高反応性脱水縮合剤及び機能性脱水縮...

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https://kaken.nii.ac.jp/search/?qm=10214975

https://kaken.nii.ac.jp/grant/KAKENHI-PROJECT-26293003/

https://kaken.nii.ac.jp/report/KAKENHI-PROJECT-26293003/26293003seika/

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Material Type: 文書・図像類
Title: 脱水縮合反応を志向した新規骨格を有する電子欠乏性含窒素芳香環の開発
Author/Editor: 國嶋, 崇隆
Kunishima, Munetaka
Author Heading: 國嶋, 崇隆
Kunishima, Munetaka
Publication Date: 2017-05-24
Publication Date (W3CDTF): 2017-05-24
Alternative Title: Development of novel pi-electron dificient nitrogen-containing heterocycles for dehydrocondensations
Periodical title: 平成28(2016)年度科学研究費補助金基盤研究(B) 研究成果報告書 = 2016 Fiscal Year Final Research Report
No. or year of volume/issue: 2014-04-01 - 2017-03-31
Volume: 2014-04-01 - 2017-03-31
Pages: 6p.-
Text Language Code: jpn
Subject Heading: 脱水縮合剤
トリアジン
電子欠乏性含窒素芳香環
アルキル化剤
Target Audience: 一般
Note (General): 金沢大学医薬保健研究域薬学系
脱水縮合剤DMT-MMは、水中やアルコール中でもカルボン酸とアミンの脱水縮合反応が選択的に進行し、アミドを高収率に与える優れた縮合剤である。今回、DMT-MMを構成するπ電子欠乏性トリアジン環の置換基検討と骨格変換を行うことで、複数の新規高反応性脱水縮合剤及び機能性脱水縮合剤を開発した。これらの知見を基に、同様にトリアジンを基盤とする新規アルキル化剤及び新規反応の開発にも成功した。
We have developed novel dehydrocondensing reagents related to DMT-MM, which enables us to conduct reactions between carboxylic acids and amines in aqueous or alcoholic solvents to give amides. In this research project, we succeeded in synthesizing highly activated and/or functionalized dehydrocondensing reagents by the detailed study on the substituent effect and the skeletal transformation of pi-electron-deficient triazines. Moreover, based on the obtained results, novel alkylating reagents and methods for chemical transformation were also developed.
研究課題/領域番号:26293003, 研究期間(年度):2014-04-01 - 2017-03-31
DOI: 10.24517/00051632
Access Restrictions: 限定公開
Related Material: https://kaken.nii.ac.jp/search/?qm=10214975
https://kaken.nii.ac.jp/grant/KAKENHI-PROJECT-26293003/
https://kaken.nii.ac.jp/report/KAKENHI-PROJECT-26293003/26293003seika/
Data Provider (Database): 国立情報学研究所 : 学術機関リポジトリデータベース（IRDB）（機関リポジトリ）
https://irdb.nii.ac.jp
Original Data Provider (Database): 金沢大学 : 金沢大学学術情報リポジトリKURA