集積型二重結合を基軸とする環化反応と天然物合成

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Author: 向, 智里ほか

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Publication date: 2015-05-25

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Note (General)：: 金沢大学医薬保健研究域薬学系集積型二重結合であるアレン及び関連π成分を基盤とする、新たな反応性の開拓並びに天然物の効率的合成法の確立を目的に研究を行い、以下の成果を得た。1)アレン―アルキン体を用いたdouble Pauson-Khand型反応の開発，2)アレン―ニトロン体を用いた1,3-双極子環化...

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https://kaken.nii.ac.jp/ja/search/?kw=70143914

https://kaken.nii.ac.jp/ja/grant/KAKENHI-PROJECT-24390003/

https://kaken.nii.ac.jp/ja/report/KAKENHI-PROJECT-24390003/24390003seika/

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Material Type: 文書・図像類
Title: 集積型二重結合を基軸とする環化反応と天然物合成
Author/Editor: 向, 智里
Mukai, Chisato
Author Heading: 向, 智里
Mukai, Chisato
Publication Date: 2015-05-25
Publication Date (W3CDTF): 2015-05-25
Alternative Title: Novel reactions and total syntheses of natural products based on cumulated double bonds
Periodical title: 平成26(2014)年度科学研究費補助金基盤研究(B) 研究成果報告書 = 2014 Fiscal Year Final Research Report
No. or year of volume/issue: 2012-04-01 – 2015-03-31
Volume: 2012-04-01 – 2015-03-31
Pages: 6p.-
Text Language Code: jpn
Subject Heading: アレン
天然物合成
1,3-双極子環化反応
Pauson-Khand型反応
ロジウム
モリブデン
Target Audience: 一般
Note (General): 金沢大学医薬保健研究域薬学系
集積型二重結合であるアレン及び関連π成分を基盤とする、新たな反応性の開拓並びに天然物の効率的合成法の確立を目的に研究を行い、以下の成果を得た。1)アレン―アルキン体を用いたdouble Pauson-Khand型反応の開発，2)アレン―ニトロン体を用いた1,3-双極子環化付加反応の開発，3)Kopsihainanine Aの不斉全合成，4)Indicanoneの不斉全合成，5)Scytoneminの炭素アナログ合成，6)Fusicoccane型三環性骨格の効率的構築法の開発.
The following six results based on allene chemistry were observed.1)Regioselective intramolecular [3+2] annulation of allene-nitrones, 2)Molybdenum-mediated intramolecular double Pauson-Khand type reaction of bis(allenyne), 3)Asymmetric total synthesis of (+)-kopsihainanine A, 4)First total synthesis of (+)-indicanone, 5)The synthesis of a carbon analogue of scytonemin based on the double Pauson-Khand type adduct, 6)Syntheses of 6-8-5 tricyclic ring systems by carbonylative [2+2+1] cycloaddition of bis(allene)s.
研究課題/領域番号:24390003, 研究期間(年度):2012-04-01 – 2015-03-31
DOI: 10.24517/00059608
Access Restrictions: 限定公開
Related Material: https://kaken.nii.ac.jp/ja/search/?kw=70143914
https://kaken.nii.ac.jp/ja/grant/KAKENHI-PROJECT-24390003/
https://kaken.nii.ac.jp/ja/report/KAKENHI-PROJECT-24390003/24390003seika/
Data Provider (Database): 国立情報学研究所 : 学術機関リポジトリデータベース（IRDB）（機関リポジトリ）
https://irdb.nii.ac.jp
Original Data Provider (Database): 金沢大学 : 金沢大学学術情報リポジトリKURA