水素化物生成-高出力窒素マイクロ波誘導プラズマ発光分光分析による鉄鋼中の鉛の定量

• 資料種別: 記事
• タイトル: 水素化物生成-高出力窒素マイクロ波誘導プラズマ発光分光分析による鉄鋼中の鉛の定量
• 著者・編者: 松本 明弘; 塩崎 唯史; 中原 武利
• 著者標目: 松本 明弘; 塩崎 唯史; 中原 武利
• タイトル（掲載誌）: 分析化学 / 日本分析化学会 編
• 巻号年月日等（掲載誌）: 53(10) 2004.10
• 掲載巻: 53
• 掲載号: 10
• 掲載ページ: 1157～1161
• 掲載年月日（W3CDTF）: 2004-10
• ISSN（掲載誌）: 0525-1931
• ISSN-L（掲載誌）: 0525-1931
• 出版事項（掲載誌）: 東京 : 日本分析化学会
• 出版地（国名コード）: JP
• 本文の言語コード: jpn
• 件名標目: high power nitrogen microwave induced plasma; atomic emission spectrometry; hydride generation method; lead; steel
• NDLC: ZP4
• 対象利用者: 一般
• コレクション（個別）: 国立国会図書館デジタルコレクション > 電子書籍・電子雑誌 > 学術機関 > 学協会; https://dl.ndl.go.jp/collections/B00043
• オンライン閲覧公開範囲: インターネット公開
• 遠隔複写可否（NDL）: 不可
• 所蔵機関: 国立国会図書館
• 請求記号: Z17-9
• 関連情報（URI）: http://dl.ndl.go.jp/info:ndljp/pid/10895916
• 関連情報（国立国会図書館永続的識別子）: info:ndljp/pid/10895916; http://dl.ndl.go.jp/info:ndljp/pid/10895916
• 連携機関・データベース: 国立国会図書館 : 国立国会図書館雑誌記事索引; https://ndlsearch.ndl.go.jp
• 書誌ID（NDLBibID）: 7121185; http://id.ndl.go.jp/bib/7121185
• 整理区分コード: 632

• 要約等: An annular-shaped high power nitrogen microwave induced plasma atomic emission spectrometry with a hydride generation method is described for the determination of lead in steel. Under the optimized experimental conditions, the best attainable detection limit at the Pb I 368.347 nm lines was 35.2 ng ml⁻¹ for lead. The linear dynamic range for lead was 100 to 30000 ng ml⁻¹ in concentrations. The presence of several diverse elements was found to cause a more or less depressing interference with the proposed technique. Of the several oxidizing agents examined, hydrogen peroxide for lead was found to be the most preferable to oxidize lead prior to hydride generation. When lead in two certified reference materials of steel was determined, a large amount of Fe(III) in the solution caused a severe depressing interference, while the presence of Fe(II) showed little or no significant interference. Of the several interference-releasing agents examined, L-ascorbic acid was found to be the most preferable to pre-reduce Fe(III) to Fe(II). The concentrations of lead in steel were determined by the use of the standard additions method. The results obtained by this method were in good agreement with their certified values.<br>
• DOI: 10.2116/bunsekikagaku.53.1157
• オンライン閲覧公開範囲: インターネット公開
• 連携機関・データベース: 科学技術振興機構 : J-STAGE; http://www.jstage.jst.go.jp

• 要約等: An annular-shaped high power nitrogen microwave induced plasma atomic emission spectrometry with a hydride generation method is described for the determination of lead in steel. Under the optimized experimental conditions, the best attainable detection limit at the Pb I 368.347 nm lines was 35.2 ng ml⁻¹ for lead. The linear dynamic range for lead was 100 to 30000 ng ml⁻¹ in concentrations. The presence of several diverse elements was found to cause a more or less depressing interference with the proposed technique. Of the several oxidizing agents examined, hydrogen peroxide for lead was found to be the most preferable to oxidize lead prior to hydride generation. When lead in two certified reference materials of steel was determined, a large amount of Fe(III) in the solution caused a severe depressing interference, while the presence of Fe(II) showed little or no significant interference. Of the several interference-releasing agents examined, L-ascorbic acid was found to be the most preferable to pre-reduce Fe(III) to Fe(II). The concentrations of lead in steel were determined by the use of the standard additions method. The results obtained by this method were in good agreement with their certified values.<br>
• DOI: 10.2116/bunsekikagaku.53.1157; https://doi.org/10.2116/bunsekikagaku.53.1157
• 関連情報（URI）: http://id.ndl.go.jp/bib/7121185; https://ndlsearch.ndl.go.jp/books/R000000004-I7121185; https://dl.ndl.go.jp/pid/10895916; http://id.ndl.go.jp/digimeta/10895916; http://www.jstage.jst.go.jp/article/bunsekikagaku/53/10/53_10_1157/_pdf; http://dl.ndl.go.jp/info:ndljp/pid/10895916
• 参照: イオン交換吸着―イオン対溶離法による鉄鋼分解液からの鉛（ＩＩ）の分離濃縮および黒鉛炉原子吸光定量; https://cir.nii.ac.jp/crid/1390001205125939968; イオン交換吸着‐イオン対溶離法による鉄鋼中のビスマス，鉛およびアンチモンの分離濃縮; https://cir.nii.ac.jp/crid/1390001205127195392; 分離・濃縮による鉄鋼微量成分分析の発展; https://cir.nii.ac.jp/crid/1390001205128158976; 鉄鋼微量成分分析における分離技術の最近の進歩; https://cir.nii.ac.jp/crid/1390001205128342400; Development of Gas-Phase Sample-Introduction Techniques for Analytical Atomic Spectrometry; https://cir.nii.ac.jp/crid/1390282679232477568
• 参照: Determination of lead at the ng ml-1 level by reduction to plumbane and measurement by inductively-coupled plasma emission spectrometry; https://cir.nii.ac.jp/crid/1360011145319503616; Determination of lead by hydride generation atomic absorption spectrometry (HGAAS) using a solid medium for generating hydride; https://cir.nii.ac.jp/crid/1360011145812062464; Evaluation of the detection capability of a high power nitrogen microwave-induced plasma for both atomic emission and mass spectrometry; https://cir.nii.ac.jp/crid/1360292619794657280; Simultaneous determination of hydride forming elements (As, Bi, Ge, Sb, Se) and Hg in biological and environmental reference materials by electrothermal vaporization–microwave induced plasma-optical emission spectrometry with their in situ trapping in a graphite furnace; https://cir.nii.ac.jp/crid/1360574096040265728; Determination of volatile hydride-forming metals in steel by atomic absorption spectrometry; https://cir.nii.ac.jp/crid/1360855568967695872; High-sensitivity microwave-induced plasma mass spectrometry for trace element analysis; https://cir.nii.ac.jp/crid/1360855571017676928; Simultaneous determination of bismuth and tellurium in steels by high power nitrogen microwave induced plasma atomic emission spectrometry coupled with the hydride generation technique; https://cir.nii.ac.jp/crid/1361137045649301376; Effect of adding oxygen gas to a high power nitrogen microwave-induced plasma for atomic emission spectrometry; https://cir.nii.ac.jp/crid/1361699994115390848; gDetermination of trace amounts of antimony in pure copper by high-power nitrogen microwave-induced plasma atomic emission spectrometry with hydride generation; https://cir.nii.ac.jp/crid/1361699996185242752; Different sample introduction systems for the multaneous determination of As, Sb and Se by microwave-induced plasma atomic emission spectrometry; https://cir.nii.ac.jp/crid/1362262944464746752; Elemental mass spectrometry using a nitrogen microwave-induced plasma as an ion source; https://cir.nii.ac.jp/crid/1362262944616633600; Matrix effects of easily ionizable elements and nitric acid in high-power microwave-induced nitrogen plasma atomic emission spectrometry; https://cir.nii.ac.jp/crid/1362262945374549504; Spatial Characterization of Emission Intensities and Temperatures of a High Power Nitrogen Microwave-induced Plasma; https://cir.nii.ac.jp/crid/1362544419087405568; Determination of trace amounts of selenium and tellurium in high-purity iron by electrothermal atomic absorption spectrometry after reductive coprecipitation with palladium using ascorbic acid; https://cir.nii.ac.jp/crid/1362544420135163008; Determination of some hydride-forming elements in urine by resin complexation and inductively coupled plasma atomic spectroscopy; https://cir.nii.ac.jp/crid/1362825893533955712; Determination of arsenic and antimony by hydride generation atomic absorption spectrometry using a small hydride generator; https://cir.nii.ac.jp/crid/1363951793809971968; Excitation Temperature in High-Power Nitrogen Microwave-Induced Plasma at Atmospheric Pressure; https://cir.nii.ac.jp/crid/1364233268205590016; Annular-shaped microwave-induced nitrogen plasma at atmospheric pressure for emission spectrometry of solutions.; https://cir.nii.ac.jp/crid/1390001204254874624; Concentrations of Hazardous Heavy Metals in Environmental Samples Collected in Xiamen, China, as Determined by Vapor Generation Non-dispersive Atomic Fluorescence Spectrometry; https://cir.nii.ac.jp/crid/1390001204257168512; 水素化物生成一高出力窒素マイクロ波誘導プラズマ発光分光分析による鉄鋼中のアンチモンの高感度定量; https://cir.nii.ac.jp/crid/1390001205183094912; 水素化物生成-高出力窒素マイクロ波誘導プラズマ発光分光分析による鉄鋼中のビスマスの定量; https://cir.nii.ac.jp/crid/1390001205184061568; 鉛の水素化物生成-原子吸光法の基礎的条件の検討及び岩石試料などへの応用; https://cir.nii.ac.jp/crid/1390282679029697152; Contents and Uptake Rates of Mn, Fe, Co, Zn, and Se in Se-Deficient Rat Liver Cell Fractions.; https://cir.nii.ac.jp/crid/1390282679234283264; 水素化物生成‐高出力窒素マイクロ波誘導プラズマ発光分光分析による鉄鋼中のヒ素，ビスマス，アンチモン及びセレンの同時定量; https://cir.nii.ac.jp/crid/1390282679330981888; 水素化ホウ素ナトリウムを用いる鉛の還元気化原子吸光法におけるニクロム酸カリウム,過酸化水素,ペルオキソニ硫酸塩,又は過マンガン酸カリウムによる増感効果; https://cir.nii.ac.jp/crid/1390282679332532352; 水素化物生成-高出力窒素マイクロ波誘導プラズマ発光分光分析による鉄鋼と高純度銅中のヒ素およびアンチモンの同時定量; https://cir.nii.ac.jp/crid/1390282680158760832; 水素化物生成-高出力窒素マイクロ波誘導プラズマ発光分光分析による鉄鋼中のヒ素およびセレンの高感度定量; https://cir.nii.ac.jp/crid/1390282680160170880; 水素化物生成-高出力窒素マイクロ波誘導プラズマ発光分光分析による鉄鋼中のヒ素,ビスマスおよびアンチモンの同時定量; https://cir.nii.ac.jp/crid/1390282680160861312
• 連携機関・データベース: 国立情報学研究所 : CiNii Research; https://cir.nii.ac.jp/
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• 書誌ID（NDLBibID）: 7121185; http://id.ndl.go.jp/bib/7121185; 10895916; http://id.ndl.go.jp/bib/10895916
• NII論文ID: 110002905327