水素化物生成-高出力窒素マイクロ波誘導プラズマ発光分光分析による鉄鋼中の鉛の定量
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- Material Type
- 記事
- Author/Editor
- 松本 明弘塩崎 唯史中原 武利
- Periodical title
- 分析化学 / 日本分析化学会 編
- No. or year of volume/issue
- 53(10) 2004.10
- Volume
- 53
- Issue
- 10
- Pages
- 1157～1161
- Publication date of volume/issue (W3CDTF)
- 2004-10
- ISSN (Periodical Title)
- 0525-1931
- ISSN-L (Periodical Title)
- 0525-1931
- Publication (Periodical Title)
- 東京 : 日本分析化学会
- Place of Publication (Country Code)
- JP
- Text Language Code
- jpn
- Subject Heading
- NDLC
- Target Audience
- 一般
- Collection (particular)
- 国立国会図書館デジタルコレクション > 電子書籍・電子雑誌 > 学術機関 > 学協会
- Access Restrictions
- インターネット公開
- Availability of remote photoduplication service
- 不可
- Holding library
- 国立国会図書館
- Call No.
- Z17-9
- Related Material (URI)
- Related Material (Persistent ID (NDL))
- info:ndljp/pid/10895916
- Data Provider (Database)
- 国立国会図書館 : 国立国会図書館雑誌記事索引
- Bibliographic ID (NDL)
- 7121185
- Bibliographic Record Category (NDL)
- 632
- Summary, etc.
- An annular-shaped high power nitrogen microwave induced plasma atomic emission spectrometry with a hydride generation method is described for the determination of lead in steel. Under the optimized experimental conditions, the best attainable detection limit at the Pb I 368.347 nm lines was 35.2 ng ml<sup>−1</sup> for lead. The linear dynamic range for lead was 100 to 30000 ng ml<sup>−1</sup> in concentrations. The presence of several diverse elements was found to cause a more or less depressing interference with the proposed technique. Of the several oxidizing agents examined, hydrogen peroxide for lead was found to be the most preferable to oxidize lead prior to hydride generation. When lead in two certified reference materials of steel was determined, a large amount of Fe(III) in the solution caused a severe depressing interference, while the presence of Fe(II) showed little or no significant interference. Of the several interference-releasing agents examined, L-ascorbic acid was found to be the most preferable to pre-reduce Fe(III) to Fe(II). The concentrations of lead in steel were determined by the use of the standard additions method. The results obtained by this method were in good agreement with their certified values.<br>
- DOI
- 10.2116/bunsekikagaku.53.1157
- Access Restrictions
- インターネット公開
- Data Provider (Database)
- 科学技術振興機構 : J-STAGE
- Summary, etc.
- An annular-shaped high power nitrogen microwave induced plasma atomic emission spectrometry with a hydride generation method is described for the determination of lead in steel. Under the optimized experimental conditions, the best attainable detection limit at the Pb I 368.347 nm lines was 35.2 ng ml<sup>−1</sup> for lead. The linear dynamic range for lead was 100 to 30000 ng ml<sup>−1</sup> in concentrations. The presence of several diverse elements was found to cause a more or less depressing interference with the proposed technique. Of the several oxidizing agents examined, hydrogen peroxide for lead was found to be the most preferable to oxidize lead prior to hydride generation. When lead in two certified reference materials of steel was determined, a large amount of Fe(III) in the solution caused a severe depressing interference, while the presence of Fe(II) showed little or no significant interference. Of the several interference-releasing agents examined, L-ascorbic acid was found to be the most preferable to pre-reduce Fe(III) to Fe(II). The concentrations of lead in steel were determined by the use of the standard additions method. The results obtained by this method were in good agreement with their certified values.<br>
- DOI
- 10.2116/bunsekikagaku.53.1157
- Related Material (URI)
- Is Referenced By
- イオン交換吸着―イオン対溶離法による鉄鋼分解液からの鉛（ＩＩ）の分離濃縮および黒鉛炉原子吸光定量イオン交換吸着‐イオン対溶離法による鉄鋼中のビスマス，鉛およびアンチモンの分離濃縮分離・濃縮による鉄鋼微量成分分析の発展鉄鋼微量成分分析における分離技術の最近の進歩Development of Gas-Phase Sample-Introduction Techniques for Analytical Atomic Spectrometry
- References
- Determination of lead at the ng ml-1 level by reduction to plumbane and measurement by inductively-coupled plasma emission spectrometryDetermination of lead by hydride generation atomic absorption spectrometry (HGAAS) using a solid medium for generating hydrideEvaluation of the detection capability of a high power nitrogen microwave-induced plasma for both atomic emission and mass spectrometrySimultaneous determination of hydride forming elements (As, Bi, Ge, Sb, Se) and Hg in biological and environmental reference materials by electrothermal vaporization–microwave induced plasma-optical emission spectrometry with their in situ trapping in a graphite furnaceDetermination of volatile hydride-forming metals in steel by atomic absorption spectrometryHigh-sensitivity microwave-induced plasma mass spectrometry for trace element analysisSimultaneous determination of bismuth and tellurium in steels by high power nitrogen microwave induced plasma atomic emission spectrometry coupled with the hydride generation techniqueEffect of adding oxygen gas to a high power nitrogen microwave-induced plasma for atomic emission spectrometrygDetermination of trace amounts of antimony in pure copper by high-power nitrogen microwave-induced plasma atomic emission spectrometry with hydride generationDifferent sample introduction systems for the multaneous determination of As, Sb and Se by microwave-induced plasma atomic emission spectrometryElemental mass spectrometry using a nitrogen microwave-induced plasma as an ion sourceMatrix effects of easily ionizable elements and nitric acid in high-power microwave-induced nitrogen plasma atomic emission spectrometrySpatial Characterization of Emission Intensities and Temperatures of a High Power Nitrogen Microwave-induced PlasmaDetermination of trace amounts of selenium and tellurium in high-purity iron by electrothermal atomic absorption spectrometry after reductive coprecipitation with palladium using ascorbic acidDetermination of some hydride-forming elements in urine by resin complexation and inductively coupled plasma atomic spectroscopyDetermination of arsenic and antimony by hydride generation atomic absorption spectrometry using a small hydride generatorExcitation Temperature in High-Power Nitrogen Microwave-Induced Plasma at Atmospheric PressureAnnular-shaped microwave-induced nitrogen plasma at atmospheric pressure for emission spectrometry of solutions.Concentrations of Hazardous Heavy Metals in Environmental Samples Collected in Xiamen, China, as Determined by Vapor Generation Non-dispersive Atomic Fluorescence Spectrometry水素化物生成一高出力窒素マイクロ波誘導プラズマ発光分光分析による鉄鋼中のアンチモンの高感度定量水素化物生成-高出力窒素マイクロ波誘導プラズマ発光分光分析による鉄鋼中のビスマスの定量鉛の水素化物生成-原子吸光法の基礎的条件の検討及び岩石試料などへの応用Contents and Uptake Rates of Mn, Fe, Co, Zn, and Se in Se-Deficient Rat Liver Cell Fractions.水素化物生成‐高出力窒素マイクロ波誘導プラズマ発光分光分析による鉄鋼中のヒ素，ビスマス，アンチモン及びセレンの同時定量水素化ホウ素ナトリウムを用いる鉛の還元気化原子吸光法におけるニクロム酸カリウム,過酸化水素,ペルオキソニ硫酸塩,又は過マンガン酸カリウムによる増感効果水素化物生成-高出力窒素マイクロ波誘導プラズマ発光分光分析による鉄鋼と高純度銅中のヒ素およびアンチモンの同時定量水素化物生成-高出力窒素マイクロ波誘導プラズマ発光分光分析による鉄鋼中のヒ素およびセレンの高感度定量水素化物生成-高出力窒素マイクロ波誘導プラズマ発光分光分析による鉄鋼中のヒ素,ビスマスおよびアンチモンの同時定量
- Data Provider (Database)
- 国立情報学研究所 : CiNii Research
- Original Data Provider (Database)
- Japan Link Center雑誌記事索引データベース雑誌記事索引データベースCrossref国立国会図書館デジタルコレクションCiNii ArticlesCrossrefCrossrefCrossrefCrossrefCrossref
- Bibliographic ID (NDL)
- 712118510895916
- NAID
- 110002905327