LC/MS/MSによるビールおよびビール原料中フモニシンB1およびB2の分析
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- Material Type
- 記事
- Author/Editor
- 須賀 啓子望月 直樹山下 博
- Periodical title
- 食品衛生学雑誌 = Food hygiene and safety science
- No. or year of volume/issue
- 45(5) (通号 258) 2004
- Volume
- 45
- Issue
- 5
- Sequential issue number
- 258
- Pages
- 255～258
- Publication date of volume/issue (W3CDTF)
- 2004
- ISSN (Periodical Title)
- 0015-6426
- ISSN-L (Periodical Title)
- 0015-6426
- Publication (Periodical Title)
- 東京 : 日本食品衛生学会
- Place of Publication (Country Code)
- JP
- Text Language Code
- jpn
- Subject Heading
- NDLC
- Target Audience
- 一般
- Holding library
- 国立国会図書館
- Call No.
- Z19-364
- Data Provider (Database)
- 国立国会図書館 : 国立国会図書館雑誌記事索引
- Bibliographic ID (NDL)
- 7140030
- Bibliographic Record Category (NDL)
- 632
- Summary, etc.
- A simple method for analysis of fumonisin B<sub>1</sub> (FB<sub>1</sub>) and fumonisin B<sub>2</sub> (FB<sub>2</sub>) in beer and raw materials of beer using liquid chromatography-electrospray ionization tandem mass spectrometry (LC/MS/MS) was developed. Samples were prepared and purified by using solid-phase extraction columns (SAX). The LC separation was performed with an octadecylated silica column at a flow-rate of 0.2 mL/min, using a mobile phase consisting of water and acetonitrile. MS/MS was used in multiple reaction monitoring, employing electrospray ionization (ESI-MRM).<br>Recoveries of spiked FB<sub>1</sub> and FB<sub>2</sub> from beer were 64% and 52%, respectively, at the level of 5 μg/kg. Recoveries of spiked FB<sub>1</sub> and FB<sub>2</sub> from malt, cornstarch, and corn grit, at the level of 50 μg/kg, were 87.9% and 86.4%, 89.5% and 87.9%, 86.6% and 81.1%, respectively. This method may have applications in quality assurance.液体クロマトグラフ/タンデム質量分析計(LC/MS/MS)によるビール，ビール原料(麦芽，コーンスターチ，コーングリッツ)およびコーンスターチの原料とうもろこし中のフモニシンB<sub>1</sub>およびB<sub>2</sub>の分析法について検討を行った．ビール試料は脱気後，陰イオン交換樹脂(SAX)で精製した．ビール以外の固体試料はメタノール-水(3 : 1)混液で抽出した後，陰イオン交換樹脂で精製した．LC/MS/MS条件はODS系カラムを用い，エレクトロスプレーイオン化マルチプルリアクションモニタリング法(ESI-MRM)を用いた．その結果，ビールで52.1～64.2%，麦芽で86.4～87.9%，コーンスターチで87.9～89.5%，コーングリッツで81.1～86.6%，とうもろこしで88.4～89.3% の回収率が得られた．
- DOI
- 10.3358/shokueishi.45.255
- Access Restrictions
- インターネット公開
- Data Provider (Database)
- 科学技術振興機構 : J-STAGE
- Summary, etc.
- 液体クロマトグラフ/タンデム質量分析計(LC/MS/MS)によるビール，ビール原料(麦芽，コーンスターチ，コーングリッツ)およびコーンスターチの原料とうもろこし中のフモニシンB<sub>1</sub>およびB<sub>2</sub>の分析法について検討を行った．ビール試料は脱気後，陰イオン交換樹脂(SAX)で精製した．ビール以外の固体試料はメタノール-水(3 : 1)混液で抽出した後，陰イオン交換樹脂で精製した．LC/MS/MS条件はODS系カラムを用い，エレクトロスプレーイオン化マルチプルリアクションモニタリング法(ESI-MRM)を用いた．その結果，ビールで52.1～64.2%，麦芽で86.4～87.9%，コーンスターチで87.9～89.5%，コーングリッツで81.1～86.6%，とうもろこしで88.4～89.3% の回収率が得られた．
- DOI
- 10.3358/shokueishi.45.255
- Related Material (URI)
- Is Referenced By
- 食の安全におけるLC-MS/MS分析の問題点分析屋目線での食の安全・安心―３ 食の安全におけるＬＣ‐ＭＳ／ＭＳ分析食の安全確保にかかわるLC-MS/MSの基本的な分析技術コメ中のフモニシンB1, B2, B3の液体クロマトグラフィーによる定量
- References
- Simultaneous Determination of Fumonisin B<sub>1</sub> and Hydrolyzed Fumonisin B<sub>1</sub> in Corn Products by Liquid Chromatography/Electrospray Ionization Mass SpectrometryOccurrence of fumonisin B<sub>1</sub>and B<sub>2</sub>in beer*Identification and determination of fumonisin FB1 and FB2 in corn and corn products by high-performance liquid chromatography-electrospray-ionization tandem mass spectrometry (HPLC-ESI-MS-MS)Determination of Fumonisins in Corn: Evaluation of Competitive Immunoassay and HPLC TechniquesQuantitative Determination of Fumonisins B<sub>1</sub>and B<sub>2</sub>by High-Performance Liquid Chromatography with Fluorescence DetectionAnalysis of Fumonisin B<sub>1</sub> in <i>Fusarium proliferatum</i>-Infected Asparagus Spears and Garlic Bulbs from Germany by Liquid Chromatography−Electrospray Ionization Mass SpectrometryAnalysis of Beer for FumonisinsQuantitation of fumonisins in corn by HPLC with o-phthalaldehyde postcolumn derivatization and their identification by LC/MSEvaluation of enzyme‐linked immunosorbent assay for analysis of beer for fumonisinsOccurrence of fumonisins in Spanish beers analyzed by an enzyme-linked immunosorbent assay method.Liquid Chromatographic Determination of Fumonisins with 4-Fluoro-7-nitrobenzofurazanFumonisins
- Data Provider (Database)
- 国立情報学研究所 : CiNii Research
- Original Data Provider (Database)
- Japan Link Center学術機関リポジトリデータベース雑誌記事索引データベースCrossrefPubMedCiNii ArticlesCrossrefCrossrefCrossrefCrossref
- Bibliographic ID (NDL)
- 7140030
- NAID
- 10014277540