Direct extraction of polysaccharides from moso bamboo (phylostachys heterocycla) chips using a mixed solvent system of an amino acid ionic liquid with polar aprotic solvent

• Material Type: 記事
• Title: Direct extraction of polysaccharides from moso bamboo (phylostachys heterocycla) chips using a mixed solvent system of an amino acid ionic liquid with polar aprotic solvent
• Author/Editor: Yue Dong; Tokio Takeshita; Hisashi Miyafuji
• Publication, Distribution, etc.: 日本 : The Chemical Society of Japan
• Publication Date: 2017-12-28
• Publication Date (W3CDTF): 2017-12-28
• Periodical title: Bulletin of the Chemical Society of Japan
• No. or year of volume/issue: 91(3)
• Volume: 91(3)
• ISSN (Periodical Title): 1348-0634
• ISSN-L (Periodical Title): 0009-2673
• Text Language Code: eng
• DOI: 10.1246/bcsj.20170383; https://doi.org/10.1246/bcsj.20170383
• Persistent ID (NDL): info:ndljp/pid/11343757; https://dl.ndl.go.jp/pid/11343757
• Collection: 障害者向け資料
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• Collection (particular): 国立国会図書館デジタルコレクション > 電子書籍・電子雑誌 > 学術機関 > 学協会; https://dl.ndl.go.jp/collections/B00043
• Acquisition Basis: オンライン資料収集制度
• Date Accepted (W3CDTF): 2019-08-28T20:45:13+09:00
• Date Captured (W3CDTF): 2019-03-13
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• Periodical Title (URI): https://www.journal.csj.jp/toc/bcsj/91/3
• Periodical Title (Persistent ID (NDL)): info:ndljp/pid/11343755; https://dl.ndl.go.jp/pid/11343755
• Data Provider (Database): 国立国会図書館 : 国立国会図書館デジタルコレクション; https://dl.ndl.go.jp

• Collection (particular): 国立国会図書館デジタルコレクション > 電子書籍・電子雑誌 > 学術機関 > 学協会; https://dl.ndl.go.jp/collections/B00043
• Access Restrictions: 国立国会図書館内限定公開
• Service for the Digitized Contents Transmission Service: 図書館・個人送信対象外
• Availability of remote photoduplication service: 可
• Holding library: 国立国会図書館
• Call No.: Z53-B35
• Related Material (URI): https://dl.ndl.go.jp/info:ndljp/pid/11343757
• Related Material (Persistent ID (NDL)): info:ndljp/pid/11343757; https://dl.ndl.go.jp/info:ndljp/pid/11343757
• Data Provider (Database): 国立国会図書館 : 国立国会図書館雑誌記事索引; https://ndlsearch.ndl.go.jp
• Bibliographic ID (NDL): 028879094; http://id.ndl.go.jp/bib/028879094
• Bibliographic Record Category (NDL): 632

• Summary, etc.: The cellulose-dissolving ability and some physical properties of mixed solvents of an amino acid IL, N-methyl-N-(2-methoxyethyl)pyrolidin-1-ium 2,6-diaminohexanoate ([P1ME][Lys]), with polar aprotic solvents, such as 1,3-dimethylimidazolidinone (DMI), N,N-dimethylformamide (DMF), dimethylsulfoxide (DMSO), and acetonitrile (CH3CN), have been investigated. The viscosity was significantly reduced by the increasing content of polar aprotic solvents, and a 1:1 mixture (molar ratio) of [P1ME][Lys] with DMF showed 91.5 cP which corresponded to less than 1/10 compared to that of the pure IL at 25 °C (1058 cP). The β values of the mixed solvents, which have the IL contents over 0.1, exhibited β-values similar to that of the pure IL. On the other hand, the π-value was dependent on the ratio of the IL content, and the pure IL had the highest π-value. We found that the mixed solvent of [P1ME][Lys] with DMF (1:1) easily dissolved the cellulose and the mixed solvent could be used to extract cellulose from moso bamboo (Phylostachys heterocycla) powder. The efficiency of the extraction of cellulose from the bamboo powder was significantly increased when a 1:1 mixture of the IL with a polar aprotic solvent was used as the extracting solvent at 60 °C; the extraction ratio of the 1:1 mixture (IL: DMF) reached twice that of the pure IL. We thus obtained cellulose in 18% (w/w) yield from the bamboo powder.
• DOI: 10.1246/bcsj.20170383; https://doi.org/10.1246/bcsj.20170383
• Rights (production): © 2018 The Chemical Society of Japan
• Related Material (URI): https://repository.lib.tottori-u.ac.jp/records/7121; http://id.ndl.go.jp/bib/028879094; https://ndlsearch.ndl.go.jp/books/R000000004-I028879094; https://dl.ndl.go.jp/pid/11343757; http://id.ndl.go.jp/digimeta/11343757; https://academic.oup.com/bcsj/article-pdf/91/3/398/56290927/bcsj.20170383.pdf
• Is Referenced By: Design of Acyl Donor for Environmentally Benign Acylation of Cellulose Using an Ionic Liquid*; https://cir.nii.ac.jp/crid/1360848658876170752; イオン液体を使用する有機合成; https://cir.nii.ac.jp/crid/1390282752322022528
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• References (URI): https://cir.nii.ac.jp/crid/1370004236987788429
• Data Provider (Database): 国立情報学研究所 : CiNii Research; https://cir.nii.ac.jp/
• Original Data Provider (Database): 学術機関リポジトリデータベース; https://irdb.nii.ac.jp; 雑誌記事索引データベース; https://ndlsearch.ndl.go.jp; Crossref; https://www.crossref.org; CiNii Articles; 科学研究費助成事業データベース; https://kaken.nii.ac.jp/ja
• Bibliographic ID (NDL): 028879094; http://id.ndl.go.jp/bib/028879094; 11343757; http://id.ndl.go.jp/bib/11343757
• NAID: 130006507063