Structural design of coordination polymers based on manganese and chromium ions bridged by oxalate ligands

• Material Type: 記事
• Title: Structural design of coordination polymers based on manganese and chromium ions bridged by oxalate ligands
• Author/Editor: Masashi Yoshitake; Kazuya Kubo; Toru Endo
• Publication, Distribution, etc.: 日本 : The Chemical Society of Japan
• Publication Date: 2015-12-04
• Publication Date (W3CDTF): 2015-12-04
• Periodical title: Bulletin of the Chemical Society of Japan
• No. or year of volume/issue: 89(3)
• Volume: 89(3)
• ISSN (Periodical Title): 1348-0634
• ISSN-L (Periodical Title): 0009-2673
• Text Language Code: eng
• DOI: 10.1246/bcsj.20150373; https://doi.org/10.1246/bcsj.20150373
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• Date Accepted (W3CDTF): 2019-08-27T20:45:33+09:00
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• Bibliographic ID (NDL): 027165363; http://id.ndl.go.jp/bib/027165363
• Bibliographic Record Category (NDL): 632

• Summary, etc.: Coordination polymers based on oxalate-bridged {[Mn^IICr^III(oxalate)₃]⁻}_∞ complexes of (DAT-2H²⁺)(DCH[18]crown-6)₂[Mn^II(CH₃OH)Cr^III(oxalate)₃]⁻₂(CH₃OH)₃ and (DABCO-H⁺)₂(DABCO-2H²⁺)[Mn^II(CH₃OH)(Cl⁻)Cr^III(oxalate)₃]²⁻₂(CH₃OH), where DAT, DABCO, and DCH[18]crown-6 denote 2,5-diaminotoluene, 1,4-diazabicyclo[2.2.2]octane, and <i>cis</i>-<i>syn</i>-<i>cis</i>-dicyclohexano[18]crown-6, respectively, were synthesized. The crystal structure of the former complex was composed of [Mn^II(Λ)(CH₃OH)Cr^III(Λ)(oxalate)₃]⁻ units, whereas that of the latter crystal was composed of [Mn^II(Λ)(CH₃OH)(Cl⁻)Cr^III(Δ)(oxalate)₃]²⁻ units. The large flexible supramolecular cation in the former provided the two-dimensional structure of [Mn^II(Λ)(CH₃OH)Cr^III(Λ)(oxalate)₃]⁻, although the two-dimensional honeycomb structure of the {[Mn^II(Δ)Cr^III(Λ)(oxalate)₃]⁻}_∞ and {[Mn^II(Λ)Cr^III(Δ)(oxalate)₃]⁻}_∞ networks are often observed for the oxalate complexes. The round-shaped DABCO molecule in the latter induced a one-dimensional chain structure of [Mn^II(Λ)(CH₃OH)Cr^III(Δ)(oxalate)₃]⁻. The former crystal showed a magnetic field dependence of magnetization typical for a spin-canting system.
• DOI: 10.1246/bcsj.20150373
• Access Restrictions: インターネット公開
• Data Provider (Database): 科学技術振興機構 : J-STAGE; http://www.jstage.jst.go.jp

• Summary, etc.: Coordination polymers based on oxalate-bridged {[Mn^IICr^III(oxalate)₃]⁻}_∞ complexes of (DAT-2H²⁺)(DCH[18]crown-6)₂[Mn^II(CH₃OH)Cr^III(oxalate)₃]⁻₂(CH₃OH)₃ and (DABCO-H⁺)₂(DABCO-2H²⁺)[Mn^II(CH₃OH)(Cl⁻)Cr^III(oxalate)₃]²⁻₂(CH₃OH), where DAT, DABCO, and DCH[18]crown-6 denote 2,5-diaminotoluene, 1,4-diazabicyclo[2.2.2]octane, and <i>cis</i>-<i>syn</i>-<i>cis</i>-dicyclohexano[18]crown-6, respectively, were synthesized. The crystal structure of the former complex was composed of [Mn^II(Λ)(CH₃OH)Cr^III(Λ)(oxalate)₃]⁻ units, whereas that of the latter crystal was composed of [Mn^II(Λ)(CH₃OH)(Cl⁻)Cr^III(Δ)(oxalate)₃]²⁻ units. The large flexible supramolecular cation in the former provided the two-dimensional structure of [Mn^II(Λ)(CH₃OH)Cr^III(Λ)(oxalate)₃]⁻, although the two-dimensional honeycomb structure of the {[Mn^II(Δ)Cr^III(Λ)(oxalate)₃]⁻}_∞ and {[Mn^II(Λ)Cr^III(Δ)(oxalate)₃]⁻}_∞ networks are often observed for the oxalate complexes. The round-shaped DABCO molecule in the latter induced a one-dimensional chain structure of [Mn^II(Λ)(CH₃OH)Cr^III(Δ)(oxalate)₃]⁻. The former crystal showed a magnetic field dependence of magnetization typical for a spin-canting system.
• DOI: 10.1246/bcsj.20150373; https://doi.org/10.1246/bcsj.20150373
• Access Restrictions: インターネット公開
• Related Material: CCDC 1437933: Experimental Crystal Structure Determination; https://cir.nii.ac.jp/crid/1880865118112336000; CCDC 1438005: Experimental Crystal Structure Determination; https://cir.nii.ac.jp/crid/1881428067921491200
• Related Material (URI): http://id.ndl.go.jp/bib/027165363; https://ndlsearch.ndl.go.jp/books/R000000004-I027165363; https://dl.ndl.go.jp/pid/11343238; http://id.ndl.go.jp/digimeta/11343238; https://academic.oup.com/bcsj/article-pdf/89/3/354/56278769/bcsj.20150373.pdf
• Is Referenced By: Creation of a Tetranuclear MnIII2MnII2 Metalloring Structure Supported by a Penicillamine-Derived Schiff-Base Ligand; https://cir.nii.ac.jp/crid/1360579813137298304; Solvent dependence of crystal structure and dielectric relaxation in ferromagnetic [MnCr(oxalate)₃]⁻ salt; https://cir.nii.ac.jp/crid/1360861707390741376; Stable Ferromagnetic Crystal of Two‐Dimensional Manganese‐Chromium Oxalate with Supramolecular Cation; https://cir.nii.ac.jp/crid/1361975839509826816
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